Monday, November 11, 2013

Determination of Plate Efficiency of Rectification Column in Refinery Operations

CATEGORY: DISTILLATION COLUMNS
International Journal of Engineering and Technology Volume 3 No. 8, August, 2013
Determination of Plate Efficiency of Rectification Column in Refinery Operations
A. Ujile, L. G. Amagbo
Rivers State University of Science & Technology, Department of Chemical/Petrochemical Engineering, PMB 5080, Port Harcourt, Nigeria.
ABSTRACT
The determination of plate efficiency of rectification column for the separation of Bonny Light Crude Oil into its fractions was studied. The atmospheric distillation column of a typical Refinery (PHRC) was used in determining the efficiencies of the bubble-cap plate of the column. It was observed that the efficiency of the plates below the feed plate varies, but above the feed plate, it increases up the top of the column and was highest at top plate. The total number of ideal and actual plates was found to be 7. The Murphree equation for plate efficiency was used to determine the overall efficiency of the column with the aid of the McCabe-Thiele diagram to be 93.9 %. This work has shown the efficiency, reliability and integrity of the plant.
Plate efficiency plays an important role in the design of distillation column. For the desired separation of mixtures to be achieved in a distillation process, the vapour leaving a plate in the column must be equal to the liquid leaving that plate. Therefore, the actual number of plates required for a particular separation duty is determined by the efficiency of the plate. This implies that any factor that causes a decrease in the efficiency of plate will definitely change the performance of the column. So, it is important to determine the efficiency of plate column before carrying out the actual construction/installation of distillation column for separation of mixture of crude oil in the refinery. By so doing, it is possible to separate crude oil mixtures that will yield the required product purity.
The objective of this work is to determine the plate efficiency of rectification column in Port Harcourt Refinery for the separation of crude oil fractions, owing to the demand for high product purity, such that when produced it will meet the required set standards, whether sale-oriented or process oriented. It is worth noting that the actual number of plates required for a particular separation duty is determined by the efficiency of the plate. Thus, any factor that causes a decrease in plate efficiency will also change the performance of the column. Plate efficiency is affected by fouling, wear and tear as well as corrosion, and the rate at which these occur depends on the properties of the liquids being processed. Thus plate should not only be designed and constructed with appropriate materials specified, but also monitored closely the reliability and performance of prevailing process design parameters.
Free Full Text Source: http://iet-journals.org/archive/2013/august_vol_3_no_8/599473137146614.pdf

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